Techniques and Experiments for Organic Chemistry by Ralph J. Fessenden
Techniques and Experiments for Organic Chemistry by Ralph J. Fessenden PDF, ePub eBook D0wnl0ad
Techniques and Experiments for Organic Chemistry begins with the common laboratory techniques. Actual syntheses are postponed until the student has gained sufficient knowledge of organic chemistry from the lecture portion of the course to understand the experiments being performed. Synthetic work follows the technique chapters of the text and begins with alkyl halide chemistry (Williamson ether synthesis and a Grignard reaction), followed by alcohol chemistry. Spectral techniques (infrared and NMR) are placed after alcohol chemistry, approximately halfway through the text. The remaining chapters are devoted to additional synthetic procedures. The text ends with a chapter on the literature of organic chemistry, an introduction to organic qualitative analysis, and a chapter of supplemental techniques. Four appendices of assorted tables and laboratory calculations conclude the text.
Contents:1. The Organic Laboratory
2. Melting Points
3. Crystallization
4. Extraction
5. Distillation
6. Introduction to Chromatography; Thin-Layer Chromatography
7. Gas-Liquid Chromatography
8. Substitution Reactions of Alkyl Halides
9. The Grignard Reaction
10. The Chemistry of Alcohols
11. Infrared Spectroscopy
12. Nuclear Magnetic Resonance Spectroscopy
13. The Chemistry of Alkenes
14. Aromatic Substitution Reactions
15. The Chemistry of Aldehydes and Ketones
16. The Chemistry of Carboxylic Acids and their Derivatives
17. Stereochemistry
18. Enolate Condensations
19. Plant Products
20. Introduction to the Chemical Literature
21. Introduction to Qualitative Organic Analysis
22. Supplemental Techniques
Appendices
Index
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